Search results for "analiza termiczna"

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The complementary structural studies of the double metal cyanide type catalysts for the ring opening polymerization of the oxiranes

2016

Przeprowadzono badania strukturalne katalizatorów dimetalocyjankowych (DMC) z dwoma rodzajami ligandów organicznych. Zaproponowano wyjaśnienie etapów przebiegu krzywych otrzymanych metodą analizy termograwimetrycznej i różnicowej kalorymetrii skaningowej (TG/DSC) badanych katalizatorów. Wykazano obecność kilku stopni związania ligandów w kompleksach DMC. Na podstawie wyników badań z wykorzystaniem absorpcji rentgenowskiej (XAS) stwierdzono, że centrum aktywne katalizatora stanowi atom cynku. W bezpośrednim sąsiedztwie atomów Zn wykryto obecność atomów Cl, natomiast w najbliższych sferach koordynacyjnych atomu Zn nie wykryto atomów tlenu.

analiza termograwimetryczna (TG)thermogravimetric analysis (TG)rentgenowska absorpcyjna spektroskopia struktury przykrawędziowej (XANES)differential scanning calorimetry (DSC)synchrotronowa absorpcyjna spektroskopia rentgenowska (EXAFS)X-ray absorption spectroscopy (XAS)extended X-ray absorption fine structure (EXAFS)analiza termicznaanaliza wydzielanych gazów (EGA)evolved gas analysis (EGA)różnicowa kalorymetria skaningowa (DSC)double metal cyanide catalysts (DMC)katalizatory dimetalocyjankowe (DMC)X-ray absorption near edge structure (XANES)thermal analysisPolimery

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PEPhysical Sciences and Engineering
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LSLife Sciences
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SHSocial Sciences and Humanities
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